NMR and EPR Spectroscopy. Papers Presented at Varian(s Third - download pdf or read online

ISBN-10: 1483213269

ISBN-13: 9781483213262

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Extra info for NMR and EPR Spectroscopy. Papers Presented at Varian(s Third Annual Workshop on Nuclear Magnetic Resonance and Electron Paramagnetic Resonance, Held at Palo Alto, California

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7. H . MISRA, Rev. Sei. Instr. 29, 590 (1958). 8. A. ABRAGAM and M. H . L. P R Y C E , Proc. Roy. Soc. A205, 135 (1951); B . B L E A N E Y and K. W . H . STEVENS, Rep. Progr. Phys. 16, 108 (1953); K . D . BOWERS and J . OWEN, Rep. Progr. , 18, 304 (1955). 9. J . E . , Proc. Roy. Soc. A240, 67 (1957). 10. R . H . SANDS, Phys. Rev. 99, 1222 (1955). 11. A. W. OVERHAUSER, Phys. Rev. 91, 476 (1953); Phys. Rev. 92, 411 (1953). 12. A. L. M C W H O R T E R a n d J . W. M E Y E R , Phys. Rev. 109, 312 (1958).

Block diagram of X-band E P R spectrometer. tion microwave impedance bridge system employing a crystal detector. 8026 Mc/gauss of applied static magnetic field, it is convenient to use X-band microwave equipment which operates between 8000 and 12,000 Mc/s and to use applied magnetic fields in the neighborhood of 3000 gauss. With a source of 300 mW of microwave power and using low audio-frequency magnetic field modula­ tion one obtains in practice the theoretical signal-to-noise ratio and may detect 5 x 10~ 12 Δ// moles of electron spins where Δ/7 is the full width of the absorption line in gauss.

7) The linear sweep provides a linear sawtooth modulation of the mag­ netic field while simultaneously driving the X-axis of the oscilloscope. This modulation produces a small change in t h e static magnetic field (Ho) a t the sample position, t h u s sweeping the field through the reson­ ance value. c. current to the coils of the electromagnet.

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NMR and EPR Spectroscopy. Papers Presented at Varian(s Third Annual Workshop on Nuclear Magnetic Resonance and Electron Paramagnetic Resonance, Held at Palo Alto, California


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