By Claudio Luchinat, Mario Piccioli (auth.), Gerd N. La Mar (eds.)
Since A. Kowalsky's first document of the spectrum of cytochrome c in 1965, curiosity within the detection, project and interpretation of paramagnetic molecules has surged, particularly within the final decade.
periods of structures have performed a key function within the improvement of the sphere: heme proteins and iron-sulfur proteins. those platforms are precise in lots of respects, considered one of that's that they comprise well-defined chromophores, each one of which might be studied intimately outdoor the protein matrix. they're the main effectively studied macromolecules, and the 1st 8 and final six of the seventeen contributions to this publication care for heme and/or iron-sulfur proteins. the center 3 chapters survey the growth on, and important promise of, more challenging structures which don't own a chromophore, yet that have however yielded extraordinary insights into their constitution.
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Piccioli, M. and Scozzafava, A (1993) 1D versus 2D 1H NMR experiments in dicopper, dicobalt superoxide dismutase: a further mapping of the active site, Gazz. Chim. tal. 123,95-100. 77. , Luchinat, C. L. (1992) Molecular dynamics simulations on HiPIP from Chomatium vinosum and comparison with NMR data, J. Am. Chem. Soc. 114, 10683-10689. 78. , Ciurli, S. and Luchinat, C. (1994) The electronic and geometric structures of iron-sulfur proteins studied through electron-nuclear hyperfine coupling, Angew.
29. L. and Santos, H. L. F. (eds), Methods in Enzymology, Academic Press, San Diego,CA 30. L. (1993) Optimization of COSY and Related Methods. Applications to lH NMR of Horse Ferricytochrome c,J. Magn. Reson. Ser. A 104, 197-202. 31. , Piccioli, M. and Tarchi, D. (1994) COSY spectra of paramagnetic macromolecules, observability, scalar effects, cross correlation effects, relaxation allowed coherence transfer, Concepts Magn. Reson. in press 32. O. (1985) Practical Aspects of Two-Dimensional Transverse NOE Sepctroscopy, J.
461-462. 76. , Piccioli, M. and Scozzafava, A (1993) 1D versus 2D 1H NMR experiments in dicopper, dicobalt superoxide dismutase: a further mapping of the active site, Gazz. Chim. tal. 123,95-100. 77. , Luchinat, C. L. (1992) Molecular dynamics simulations on HiPIP from Chomatium vinosum and comparison with NMR data, J. Am. Chem. Soc. 114, 10683-10689. 78. , Ciurli, S. and Luchinat, C. (1994) The electronic and geometric structures of iron-sulfur proteins studied through electron-nuclear hyperfine coupling, Angew.
Nuclear Magnetic Resonance of Paramagnetic Macromolecules by Claudio Luchinat, Mario Piccioli (auth.), Gerd N. La Mar (eds.)