Download e-book for iPad: Processing, properties, and design of advanced ceramics and by Singh, Gurpreet

By Singh, Gurpreet

ISBN-10: 1119323304

ISBN-13: 9781119323303

ISBN-10: 1119323649

ISBN-13: 9781119323648

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A) (b) (c) Figure 14. TEM micrographs for oxides at 900oC: a. Mg/Fe=1:3, b. Mg/Fe= 2:1, c. Mg/Fe 5:2. CONCLUSIONS Pyroaurite-like structures with various Mg/Fe molar ratios have been obtained by coprecipitation. Structural, morphological and surface properties were found to be very dependent of the cation ratios. The Fe(III)-rich sample was mainly consisting of an amorphous Fe(III)-phase that led to oxides with very low surface area, while the samples with higher Mg(II) content consisted of crystalline pyroaurite lead to oxides with high surface area.

For the other two samples, BET values increased after heat treatment at 550oC (sample with Mg/Fe ratio 5:2) or remained about the same for the sample with Mg/Fe ratio 2:1 (Table III). As expected, all BET values decreased for the oxides at 900oC, due to the increase in crystallite size. Figure 11. Particle size distribution for all samples: a. pyroaurite, b. oxides at 900oC. 26 · Processing, Properties, and Design of Advanced Ceramics and Composites Investigation of Pyroaurite-Type Anionic Clay-Derived Mixed Oxides One of the most interesting aspects of the anionic clays, including pyroaurite, is the formation of oxides with small crystallite size and high surface area8 due to their special decomposition mechanism9, which is the best illustrated by sample with Mg/Fe ratio 5:2.

At 550oC, particles for the sample Mg/Fe ratio 1:3 become more defined in shape (Figure 13 a). The sheet-like structure for samples with Mg/Fe 2:1 and 5:2 is preserved at this temperature (Figure 13 b,c), even though the pyroaurite has decomposed in the corresponding oxides. This preservation of shape is most likely due to the topotactic decomposition mechanism9 of pyroaurite. At 900oC, rhombohedral particles are predominant for all samples, owing to rhombohedral shape of either hematite or spinel structures (Figure 14).

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Processing, properties, and design of advanced ceramics and composites by Singh, Gurpreet

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